Chemical Kinetics

Amarnath K

June 2024

Remember to ALWAYS use ICE table to simplify the reaction stoichiometry, concentrations, find degree of dissociation and such quantities in chemical kinetics AND chemical and ionic equilibrium.

Rate

For a reaction, the rate in which a product is formed, or the reactants are consumed is generally proportional to some power of the concentration of the reactant. Take a reaction

\[\ce{A -> B}\]

Here, the rate of the reaction is proportional to \([\ce A]^n\), so

\[\text{rate} = k[\ce A]^n\]

average and instantaneous rate

The average rate of the reaction is the macroscopic change in concentration of reactant (\(\Delta c\)) or product over the time it took for that change, as

\[\text{rate}=\frac{\Delta c}{\Delta t}\]

The instantaneous rate is the derivative of the concentration w.r.t time, as

\[\text{rate}_\text{inst}=\frac{dc}{dt}\]

stoichiometry in rate

For a reaction

\[\ce{aA + bB -> cC + dD}\]

The rate of the depletion of A by \(a\) is equal to that of B by \(b\) and appearance of C by \(c\) and D by \(d\). Then, the rate of the reaction is

\[\text{rate of reaction} = -\frac{d[\ce A]}{dt}\frac1a=-\frac{d[\ce B]}{dt}\frac1b=\frac{d[\ce C]}{dt}\frac1c=\frac{d[\ce D]}{dt}\frac1d\]

gas phase reaction

For a homogeneous gas-phase reaction, the rate of the reaction can be expressed in terms pressure. From \(pV=nRT\), we get \(p=cRT\), then \(c=p/RT\). This yields

\[\text{rate of reaction} = -\frac{dp_\ce A}{dt}\frac1a=-\frac{dp_\ce B}{dt}\frac1b=\frac{dp_\ce C}{dt}\frac1c=\frac{dp_\ce D}{dt}\frac1d\]

Law of mass action (Guldberg and Waage)

It states that

the rate of a reaction is directly proportional to the active mass of reactants raised to the power of their stoichiometric coefficients.

For a reaction

\[\ce{aA(g) + bB(g) -> cC(g) + dD(g)}\]

\[\text{rate}=k[\ce A]^a[\ce B]^b\]

This rate is the theoretical rate.

active mass

In certain reactions only is the experimental rate equal to the theoretical rate.

Rate law expression

It is based on the law of mass action, but instead of the stoichiometric coefficients, substitute experimentally determined variables instead, as

\[\text{rate}_E=k[\ce A]^x[\ce B]^y\]

In reactions where theoretical rate is the same as the experimental rate, both \(x,y\) and \(a,b\) become equal.

rate constant

The rate constant \(k\) of a reaction is the rate of the reaction when the concentration of all the reactants is unity (1).

Characteristics of the rate constant:

  1. It gives an idea about the speed of the reaction.
  2. every reaction has a particular rate constant at a particular temperature.
  3. It increases with temperature.
  4. It is independent of the concentration of the reactants.

The rate constant can never decrease with increase in temperature.

Classification of reactions

  1. Elementary: These reactions are single step reactions where the law of mass action holds. The theoretical rate is the same as experimental rate here.
  2. Complex: These are reactions which are completed in multiple steps only, where each step is an individual elementary reaction. The slowest step is the rate determining step. For example\[\ce{2NO + Br2 -> 2 NOBr}\]Here the steps are as follows
    1. \(\ce{NO + Br2 -> NOBr2}\)
    2. \(\ce{NO + NOBr2 -> 2NOBr}\)

Molecularity

It is a theoretical concept, the total number of reacting species which must collide simultaneously to give products.

For example:

  1. \(\ce{CaCO3 ->[\Delta] CaO + CO2}\), here the wall acts a collision medium, so molecularity is 1.
  2. \(\ce{H2 + I2->2HI}\), molecularity 2.
  3. \(\ce{2HI -> H2 + I2}\), molecularity 2.
  4. \(\ce{2NO2 + O2 -> 2NO2}\), molecularity 3. DO NOT use law of mass action in this case, since it is a complex reaction.

It can

  1. never be 0, a fraction or a negative number, i.e., \(M\in \mathbb N\).
  2. be defined only for elementary reactions.
  3. usually not go above 3. This is because the probability of three effective collisions happening simultaneously is very low.

molecularity within complex reactions

While complex reactions by themselves cannot have a molecularity, their individual steps can. For example, in the reaction given in the section classification of reactions, the individual steps have molecularity 2 and 2 respectively.

Importantly, for finding molecularity, the stoichiometric coefficients of all reactants and products must be a natural number, i.e., for \(\ce{1/2 H2 + 1/2 I2 -> HI}\), multiply the entire reaction twice to get molecularity 2.

Order of reaction

The order of the reaction is the sum of the powers of the concentration terms involved in the rate law expression.

For a reaction

\[\ce{a A + b B -> products}\]

Let the rate law expression be

\[r=k[\ce A]^x[\ce B]^y\]

Then, the order of the reaction w.r.t A is \(x\) and B is \(y\). The overall order of the reaction is \(x+y\). This must always be greater than 0, while the individual orders can be negative.

significance of order

The order of a reaction tells us how much the rate of a reaction changes on changing the concentration of the reactants.

Zero order reactions

The reactions where the rate of the reaction is completely independent of the concentration of the reactants are called zero order reactions.

For a reaction

\[\ce{A -> B}\]

The rate law expression is

\[r=k\]

Order of reaction is 0, so \(r=k[\ce A]^x\) becomes \(r=k[\ce A]^0\). From this, it can be found that \(k=-d[\ce A]/dt\), then multiply both sides by a \(dt\) and integrate to get \([\ce A]^{A_t}_{0}=-kt\). This solves to give

\[A_t=A_0-kt\label{eq1}\tag{i}\]

half life

The half life (\(t_{0.5}\) or \(t_{1/2}\)) is the time taken for half of the reaction to complete, i.e., for the concentration of the reactant to become half of its initial concentration. For \(A_t=A_0\), it can be solved from (\(\ref{eq1}\)) that

\[t_{1/2}=\frac{A_0}{2k}\]

completion time

The time taken to complete 100% of a reaction. This is easily found to be \(2t_{1/2}\) for a zero order reaction, or

\[t_{1}=2t_{0.5}=\frac{A_0}{k}\]

degree of dissociation

The degree of dissociation \(\alpha\) is the number of moles dissociated (\(A_0-A_t\) in 1L) over the total number of moles (\(A_0\)). Substituting \(A_t\) for (\(\ref{eq1}\)), we get

\[\alpha =\frac{kt}{A_0}\]

unit of the rate constant

The unit of the rate constant for a zero order reaction is \(\mathrm{mol~L^{-1}~s^{-1}}\).

NOTE: If in equal time intervals, the change in concentration of reactants remains the same, then it is a zero order reaction.

rate vs. concentration is a straight line with slope 0, since it is constant.

concentration (y) vs time (x) (i made a mistake)
half life vs concentration
completion time vs concentration
degree of dissociation vs concentration

examples of zero order reactions

  1. Photochemical reaction between H and Cl, \[\ce{H2 + Cl2 ->[h\nu] HCl}\] The rate of this reaction is k(intensity of light).
  2. Decomposition of HI on gold surface, \[\ce{2HI -> H2 + I2}\] The rate of this reaction is \(k[\ce{HI}]^0\)
  3. Decomposition of gaseous ammonia on the surface of Pt or Mo, \[\ce{2NH3 -> N2(g) + 3H2(g)}\]

First order reaction

A reaction where the rate depends linearly on the concentration of the reactant is called a first order reaction.

For a reaction

\[\ce{A -> B}, x=1\]

Let \(A_0\) be the initial concentration of the reactant and \(A_t\) be the final concentration. The rate law expression for this reaction is

\[k[\ce A] = -\frac{d[\ce A]}{dt} \implies k\int dt=-\int\frac{d[\ce A]}{[\ce A]}\]

This equation solves to give

\[\ln A_t = \ln A_0 - kt\label{eq2}\tag{ii}\]

Graphing \(\ln A_t\) against \(t\) gives a straight line with slope \(k\) (negative) and \(y\)-intercept \(\ln A_0\) as given below.

\ln A_t vs t

Convert the equation to base 10 logarithm using 2.303. Also, solve to get

\[k=\frac{1}{t}\ln\left(\frac{A_0}{A_t}\right)\quad \text{OR} \quad k=\frac{2.303}{t}\log_{10}\left(\frac{A_0}{A_t}\right) \label{eq3}\tag{iii}\]

This also yields

\[\frac{A_t}{A_0}=e^{-kt}\]

graphs

I’ve already graphed equation (\(\ref{eq2}\)) in this section.

\log_{10} A_t vs t
concentration (reactant) vs time
rate of reaction vs concentration (reactant)

half life

From the equation (\(\ref{eq3}\)), we may substitute \(A_t=A_0/2\) to get

\[t_{1/2}=\frac{\ln 2}{k}\implies t_{1/2}=\frac{0.693}{k}\]

This equation tells us that the half life of a first order reaction is independent of the initial concentration of reactant. It is only dependent on the rate of the reaction.

completion time

From the equation (\(\ref{eq3}\)), we may substitute \(A_t=0\) which gives a 0 as the denominator, and as such

\[t_1=\infty\]

The reaction will never complete, therefore it is a reversible reaction, which has its own equilibrium constant (\(K_c\)).

degree of dissociation

Drawing the ICE diagram for the reaction \(\ce{A -> B}\),

time \(\ce{A}\qquad \to\) \(\ce{B}\)
\(t=0\) \(A_0\) \(0\)
\(t=t\) \(A_t\) \(B_t\)

We know that \(\alpha = (A_0-A_t)/A_0\). For \(A_t=A_0e^{-kt}\), we get

\[\alpha = 1-e^{-kt}\]

The degree of dissociation is independent of initial concentration of reactant.

concentration of reactant left after n half lives

The number of half lives is \(t/t_{0.5}\), so then the amount of reactant left after \(n\) half lives becomes

\[A_{\text{unused}}=\frac{A_0}{2^n}\]

examples of first order reaction

  1. Halogenation of ethene \[\ce{C2H4 + H2 -> C2H6}\] The rate of reaction is \(k[\ce{C2H4}]\)
  2. All artificial and natural radioactive decay of unstable nuclei. For example \[\ce{^{226}_{88} Ra -> ^4_2 He + ^{222}_{86} Rn}\]
  3. Decomposition of \(\ce{N2O5}\) and \(\ce{N2O}\).

change of concentration w.r.t time

For a zero order reaction, for the same time intervals, the difference in concentrations is always equal. In first order reactions, it is the final over initial concentration that is constant, as

\[\frac{A_2}{A_1}=\frac{A_4}{A_3}\]

gas phase reactions

From \(pV=nRT\), it is known that \(p\propto n\). For a reaction \(\ce{A(g) -> B(g) + C(g)}\), drawing the ICE table,

time \(\ce{A(g)}\qquad \to\) \(\ce{B(g)}\qquad +\) \(\ce{C(g)}\)
\(t=0\) \(p_0\) \(0\) \(0\)
\(t\) \(P_0-x\) \(x\) \(x\)

From Dalton’s Law, we state that \(p_T=\sum p\). For \(t=0\) then, we have \(p_T=p_0\). At \(t=\infty\), we have \(p_T=2p_0\), which we can rewrite as \(p_\infty=2p_0\) (since A gives B and C with same stoichiometric coefficients).

Since \(p\propto n\), and concentration is basically the number of moles per unit substance (volume, mass, etc.), we substitute the concentration terms with pressure terms, then equation (\(\ref{eq3}\)) becomes

\[k=\frac{1}{t}\ln\left(\frac{p_0}{p_0-x}\right)\]

To remove the \(x\), we look back at the ICE table, where we find that \(p_T\) at \(t\) is \(p_T=p_0-x+x+x=p_0+x\). This allows us to find \(x\) as \(p_T-p_0\). Substitute to get

\[k=\frac1t\ln\left(\frac{p_0}{2p_0-p_T}\right)\]

In terms of \(p_\infty\) and \(p_T\), the equation becomes

\[k=\frac1t\ln\left(\frac{p_\infty}{2[p_\infty-p_T]}\right)\]

Parallel first order reactions

The reactions in which the reactant is involved in more than one first order reaction are called parallel first order reactions.

parallel first order reaction representation

In parallel first order reactions, the average rate constant

\[k_\text{avg}=k_1+k_2\]

If there are more than two rate constants, then just add them as well. This new constant can be used in all equations that are followed by first order reactions. For example, we may use equation (\(\ref{eq3}\)) here as:

\[k_1+k_2=\frac{1}t\ln\left(\frac{A_0}{A_t}\right)\]

This would also solve to become

\[A_t=A_0e^{-(k_1+k_2)t}\]

percentage of products

Take the reaction given in the above section.

Here, the percentage of B formed is

\[\%\ce B=\frac{k_1}{k_1+k_2}\times 100\]

The percentage of C formed is

\[\%\ce C=\frac{k_2}{k_1+k_2}\times 100\]

number of moles formed

Take the reaction given in the above section.

Here, the number of moles of B formed is

\[n_\ce B = \frac{k_1}{k_1+k_2}\times x\]

where \(x\) is \(A_0-A_t\) of the reactant.

The number of moles of C formed is

\[n_\ce C = \frac{k_2}{k_1+k_2}\times x\]

calculation of average half life

Since \(t_{0.5}=0.693/k\), for \(k=k_1+k_2\) we have

\[t_{0.5}=t_{{0.5}_1}+t_{{0.5}_2}\]

Order of reaction from half life

For a zero-order reaction, \(t_{0.5}\propto A_0\), and for a first order reaction it is not dependent. It can then be proven that for a reaction

\[\ce{A -> B}\]

where \(A_1\) is the concentration of reactant at \(t_{{0.5}_1}\) and \(A_2\) at \(t_{{0.5}_2}\),

\[\frac{t_{{0.5}_1}}{t_{{0.5}_2}}=\left(\frac{A_1}{A_2}\right)^{1-n}\]

where \(n\) is the order of the reaction.

Sequential reaction

The reaction which proceeds from reactants to final products through intermediate stages.

\[\ce{A ->[$k_1$] B ->[$k_2$] C}\]

Rates for each step differ as \(k[\ce A]\), \(k[\ce B]\) and so on.

Pseudo order reaction

The reaction whose order is different from the actual order due to large concentration of one of the reactants is called a pseudo order reaction.

\[\ce{A + B -> Products}\]

Then, rate \(k[\ce A][\ce B]\), when B is in excess becomes \(k'[\ce A]\).

Examples

  1. Hydrolysis of ester \[\ce{CH3COOC2H5 + H2O ->[H+] CH3COOH + C2H5OH}\] where water is present in excess, the rate becomes \(k'[\ce{CH3COOC2H5}]\).
  2. Inversion of cane sugar \[\ce{C12H22O11 + H2O ->[H+] Glucose + Fructose}\] where the rate of the reaction is \(k'[\ce{C12H22O11}]\).

These above are pseudo first order reactions.

Activated state complexes and activation energy

this is all i have written at the moment.